Allen J. Hall

Materials Science & Engineering, Productivity, and Life

Research Work

NY-PBS Captures The Struggle Of The Graduate Student

It’s not often that someone goes about deciding to make a film about graduate studies. It just so happens that Thirteen (PBS-NY) has done just that. Their film “Naturally Obsessed: The Making Of A Scientist” is quite an excellent snap-shot of the struggle of graduate students to get their PhD degree and accomplish something very difficult. Of course each of our struggles is unique. We are all dealing with our own situations, with our own fields (some not even in laboratories- the horror- is that real science? hahahah).

Speaking of our own struggles, what most of the public often does not get a feel for is the absolute devotion, almost to insanity, towards finding the solutions we are looking for. Many of the comments by the graduate’s spouses touched home for me. In each of the graduates followed in this film I saw bits of myself. One thing however, that is different, is the struggle for the specific protein structure. Often that struggle is a lot less well-defined. In this situation, you either get the structure of AMPK or you don’t. I guess it’s a lot like their attempts at creating crystals. Sure, you get crystals, but if they don’t have a periodic structure, you’ll never get diffraction. In my situation, the variables in our studies are very difficult to control, and so often one doubts one’s work solely on the question of reproducibility. Many scientists struggle with this same situation. People think that doing things like “measuring temperature” is a very easy thing. In reality, it is a very very difficult thing. Especially in a vacuum. :) That question just arose the other day in discussing our science with a new undergraduate assistant. As we talked more and more on the difficulties of measuring temperature we all saw his eyes grow larger in wonder. The simplest of problems can often be the most difficult. How accurate do you need to measure it? What standard will you use? Do you believe your thermocouple, your thermometer, or your pyrometer? What if the emissivity of the surface changes? :)

This is the life of a scientist. And the film below attempts to capture the lives and struggles of a few graduate students who are hoping for a career in science. It’s a struggle. But, you have heard me say that enough. ;) To learn more about it I strongly suggest you watch this film. For the graduate student, I warn you: you’ll see yourself in this. For those who aren’t scientists: this may end up being a comedy, and I kindly refer you to Marg Simpson’s commentary on graduate students posted earlier in this blog.

My congratulations to Thirteen for doing such an excellent job on this one hour film. They didn’t have a lot of time to share with you everything regarding our struggles and achievements, but they distilled it quite well in the time available.

MATLAB and reciprocal space mapping - small update.

Well, I’m one of those guys who believes a picture is usually worth a ton of words. I’ve got a few images to share here on the matlab code I’ve been working on for reciprocal space mapping in MATLAB. I’m still not 100% on my code right now, so I’m not sharing it for the time-being. In particular, I use an import function for .x00 slices for two-axis scans in the Panalytical/Philips XPert system. If you are using XRDML, skip the files for .x00 import that I have in other posts on this blog. In anycase, without much explanation here are the images…

surfacetestusingallomegas2

surfacetestusingallomegas3

qspaceorigtranslateweachomegaload

Software For Scientists: Engauge Digitizer

In the time I’ve been doing my research work at the Univ. of IL, I’ve come across a number of graphs from various past researchers, older papers, stuck on the side of machines (calibration curves), and even hand-drawn or chart-recorder graphs in my numerous projects.  The only major problem with those graphs I’ve found is that they aren’t in a digital form for further use with other data (instrument response functions) or to include in your own work as a reference.  So, what to do?

Well, there’s an easy solution.  It’s not the perfect solution, as it’s a bit slow, I’ll get to that in a second, but it’s a great solution to the problem, and has worked for me a number of times now.  To top it off, it’s open-source, donation-ware, and cross-platform: Engauge Digitizer (see post at LifeHacker.com).  Don’t let the website and lack of recent updates deter you.  Tools that can do what Engauge does are few and far between.  So, it is definitely worth a try.  Here’s an example of how I’ve used it just the other day (prompting this post- I’ve used it for years now, but the recent use reminded me I should share it with others).  [click "More" to see an example use and learn more]

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Filmetrics Rocks- iPod Touch 32g!!

Boston rocked: I’m writing this on a new iPod Touch! Filmetrics was running a drawing for those who brought samples to test! Big thankyou’s go out to Filmetrics and AVS. I will write more about the conference in a series of posts coming soon. I’m hoping everyone had a great week while I was gone.

AVS-Boston next week!

The society formerly known as the American Vacuum Society (AVS) is holding their international conference in Boston, MA next week! And I’ll be there! [Exciting!] If you are going to be there, drop me a line on the blog and we can snag a coffee or beer together.

The programs and cards sent out may have a familiar image! :)

My AFM image of the CuInSe2 Bicrystals I grow in our lab won second place in the Art-Zone competition last year! It was great fun! [Thanks goes to AVS for being a fantastic organization!]

AVS ArtZone Second Prize Winner- CuInSe2 Bicrystal

Wish me luck with my talk!! :)

Painful to work with- Science Direct

One thing I find extremely helpful in my research, is the ability to download citations for articles my co-workers send. I like to import them into BibDesk and auto-file the journal articles by first-author. Unfortunately, not everyone has Bibtex export abilities. This isn’t too bad, as BibDesk imports most major citation files. One thing that I do abhorr, is when a major company decides not to offer a citation download option! Science Direct is the fellow who gets my wrath this evening. It’s so bad I’ve been looking for other companies who keep track of journals that have downloads for the ones that Science Direct publishes!

I wonder if you pay their absurd journal prices, if you get citation downloads…

For more on Absurd Journal pricing, see: Knuth and “Trapped…”

Published in the Journal of Applied Physics…

Well, I’m finally published in my current field.  It took a very very long time to get this paper published.  All sorts of reasons for the delay.  In fact, this work was originally started in 2004  (our first bicrystal was successfully grown in ‘04).  During research group meeting, I made an under the breath comment something akin to: “Well, darnit, it’s too bad we can’t study a single grain-boundary, because then everything would be so much easier…”  Prof. Rockett looked over to me and smiled: “But, Allen, we can study a single grain-boundary!  That’s a great idea!”  So, the bicrystal project was started.

We were able to obtain a bicrystal GaAs wafer from Wafer Technology Limited Co. (UK); I requested a bad growth, with crystallites as large as possible.  I’ll be forever indebted to the great guys at Wafer Technology for their quick grasp of what I was looking for.  After visiting our group in 2006, S. Seibentritt at HMI (now at Lüxenbourg) started similar work.

While this current paper isn’t perfect, it went through numerous revisions.  Most of the extensive EBSD calculations didn’t make the paper.  Subsequent papers will likely revisit the disorientation discussion.

Epitaxial growth of very large grain bicrystalline Cu(In,Ga)Se2 thin films by a hybrid sputtering method
J. Appl. Phys. 103, 083540 (7 pages) (2008)

http://link.aip.org/link/?JAPIAU/103/083540/1

Unfortunately, there was an error we missed in the proof.  The paper is currently missing Figure 2(c): The cross-sectional HRTEM image (the hard work of C. Lei).  The image can be found here: Cross-Sectional HREM image of Cu(In,Ga)Se2 bicrystal, hosted at Prof. Angus Rockett’s research group’s webpage.

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A Quick Introduction...

I'm a graduate student (PhD Candidate) at the University of Illinois at Urbana-Champaign. I've studied and researched in two fields of Materials Science and Engineering (Polymers and Semiconductors). My interests are as diverse as my musical tastes and I usually have my hand in some crazy project during my free time. I'm available for consulting and have access to a world-renown materials research user-facility supported by the D.O.E. If you would like to know more, please contact me.

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